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$Non-Ideal Data Diffraction in the Real World$

Non-Ideal Data Diffraction in the Real World

Non-Ideal Data Diffraction in the Real World. Scott A Speakman, Ph.D. speakman@mit.edu http://prism.mit.edu/xray. The calculated diffraction pattern represents the ideal X-ray powder sample. The ideal powder sample Millions of grains Randomly oriented grains Flat Smooth surface

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Sticking out needle from perspex tube has less effect than increasing distance

position. distance. Linear time dependence. Distance: less than 1/r 2 !. Position: less important. Extra oxygen, no radical increase. Use of a fluorescent probe to detect radicals formed by the plasma needle

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Non-Ideal Data Diffraction in the Real World

Sticking out needle from perspex tube has less effect than increasing distance